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Under the optimized conditions, using Tween 80 (3% v/v in anolyte), peroxydisulfate (10% w/v in catholyte), and CaMnO 3 activator (0.625 g/L added to the cathode chamber) at an applied current of 1 DC Volt/cm for seven days, the mean PCB removal efficiency achieved was 51.42%

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Purified product was subjected to NMR analysis and analysis using chiral analytical HPLC with a CHIRALPAK IA-3 column (150 4.6 mm, 3 m) at room temperature (flow rate 1 ml min 1 , 40% acetonitrile in H 2 O with 0.1% trifluoroacetic acid)